Advances in Carbohydrate Chemistry, Vol. 6 by Claude S. Hudso (ed.), Sidney M. Canto (ed.)

By Claude S. Hudso (ed.), Sidney M. Canto (ed.)

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62, 2791 (1929). (69s) Violet E. Sharp and M. Stacey, J . Chem. ,285 (1951). (60) R. K. Ness, H. G. , and C. S. Hudson, J . Am. Chem. ,72, 2200 (1950). (61) C. D. Hurd and R. P. Holysr, J . Am. Chem. ,72, 2005 (1950). (62) W. W. Pigman and R. M. , New York, p. 160 (1948). (63) L. F. Fieser and Mary Fieser, “Organic Chemistry”; D. C. , p. 154 (1944). (64) C. S. Hudson, J . Am. Chem. ,46, 462 (1924). , 1, 118 (1945). arabinose is the same a8 for a-D-galactose. C. 8. Hudson and F. P. Phelps, J .

8. Hudson, J . Am. Chem. , 88, 1571 (1916). 40 W. L. EVANS, D. D. REYNOLDS AND E. A. TALLEY A number of years later, Schlubach and Maurer4*tried a number of modifications with the idea that an acid catalyst might cause the alpha configuration to predominate and give them the natural trehalose, since alkaline catalysts seemed to give the beta derivatives. They first tried treating a benzene solution of the D-glucose tetraacetate with hydrogen chloride, then tried an addition of calcium chloride, and they also melted the glucose tetraacetate with and without zinc chloride, but in no case could an a,a-trehalose derivative be isolated.

43) W. N. Haworth and Grace C. Leitch, J . Chem. ,llS, 188 (1918). (44) W. Charlton, W. N. Haworth and W. J. Hickinbottom, J. Chem. ,1527 (1927). (Ma) W. N. Haworth, J. V. Loach and C. W. Long, J . Chem. ,3146 (1927). (45) J. K. N. Jones and F. , 4, 243-291 (1949). (46) W. N. Haworth, E. L. Hirst and J. A. B. Smith, J . Chem. , 2659 (1930). 6 +go. 2 51 (21 hrs. Schlubach and K. , 66, 1957 (1923). (48) J. C. Irvine and D. McNicoll, J . Chem. , 97, 1449 (1910). (49) E. Baldwin and D. J. Bell, J .

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